Animal and vegetable fats and oils. Determination of fatty-acid-bound chloropropanediols (MCPDs) and glycidol by GC/MS - Method using acid transesterification and measurement for 2-MCPD, 3-MCPD and glycidol Ingestion-build-258901 Procedures for dose assessment based

Procedures for dose assessment based on reference levels for special monitoring program

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BS EN 61360‑6 includes the following subjects:

2 on crush resistance of rubber and plastic hoses and hoses assemblies is for:

Animal and vegetable fats and oils. Determination of fatty-acid-bound chloropropanediols (MCPDs) and glycidol by GC/MS - Method using acid transesterification and measurement for 2-MCPD, 3-MCPD and glycidol Ingestion-build-258901 Procedures for dose assessment based1 Scope This document specifies a procedure for the simultaneous determination of 2 MCPD esters (bound 2 MCPD), 3MCPD esters (bound 3MCPD) and glycidyl esters (bound glycidol) in a single assay, based on acid catalysed ester cleavage and derivatization of cleaved (free) analytes with phenylboronic acid (PBA) prior to GC MS analysis. This document is applicable to solid and liquid fats and oils. For all three analytes the limit of quantification (LOQ)